A Comparative Evaluation of the Bond Strength of Universal Resin Luting Cement and Self-adhesive Resin Luting Cement to Zirconia-reinforced Glass Ceramics: An in vitro Study
Main Article Content
Abstract
Background: Dental resin cements are widely used for luting indirect restorations, such as ceramic or zirconia crowns, veneers, and inlays, due to their superior mechanical properties and adhesive capabilities. The efficacy of bonding to zirconia and glass ceramics varies by cement type.
Aim: To evaluate and compare the bond strength of universal resin luting cement and self-adhesive resin luting cement, with surface-treated zirconia reinforced glass ceramic.
Materials and methods: Twenty CAD-CAM-milled and fully sintered zirconia-reinforced glass-ceramic (ZGC) blocks of 12 X 14 X 2 mm were prepared. Each specimen was embedded in self-cure acrylic resin cylinders, with one surface exposed for bonding. The specimens were randomly divided into two groups with 10 in each. The specimens in groups 1 and 2 were luted with self-adhesive resin cement and universal resin cement, respectively. The specimens were mounted on the universal testing machine, and the debonding chisel was allowed to make contact with the interface of the luting agent and the ceramic. Then, the load was applied at a crosshead speed of 1mm/min at the interface. The debonding load was recorded in newtons, and the shear bond strength was calculated in MPa. Overall comparisons were analyzed using the Kruskal-Wallis test. Pairwise comparisons were done using the Mann-Whitney U test. The level of significance was set at p < 0.05 for all tests.
Results: Universal resin cement demonstrated a significantly higher mean bond strength (6.94 ± 0.55 MPa) compared to self-adhesive resin cement (5.54 ± 1.09 MPa) with the surface-treated ZGC blocks. Intergroup comparison revealed a statistically significant difference in bond strength between the tested resin cements (p = 0.002).
Conclusion: Universal resin cement demonstrated the highest bond strength, whereas self-adhesive resin cement showed the lowest bond strength to the tested ceramic substrate.
Article Details
Section

This work is licensed under a Creative Commons Attribution 4.0 International License.
This work is licensed under a Creative Commons Attribution 4.0 International License.
How to Cite
References
1. Shearer A, Montazerian M, Deng B, Sly JJ, Mauro JC. Zirconia-containing glass-ceramics: From nucleating agent to primary crystalline phase. Chem Eng Sci X. 2024;6(2):e10200. https://doi.org/10.1002/ces2.10200
2. Zarone F, Di Mauro MI, Ausiello P, Ruggiero G, Sorrentino R. Current status on lithium disilicate and zirconia: A narrative review. BMC Oral Health. 2019;19(1):134. https://doi.org/10.1186/s12903-019-0838-x
3. Junior LRD, Baroudi K, Miranda ME, Vitti RP, Brandt WC. Bond strength of self-adhesive resin cement to dentin using different adhesion protocols. J Clin Exp Dent. 2022;14(1):e35-9. https://doi.org/10.4317/jced.59043
4. De Souza G, Braga RR, Cesar PF, Lopes GC. Correlation between clinical performance and degree of conversion of resin cements: A literature review. J Appl Oral Sci. 2015;23(4):358-68.
5. Arrais CA, Giannini M, Rueggeberg FA, Pashley DH. Microtensile bond strength of dual-polymerizing cementing systems to dentin using different polymerizing modes. J Prosthet Dent. 2007;97(2):99–106. https://doi.org/10.1016/j.prosdent.2006.12.007
6. Şenol M, Gürbüz A, Oyar P. Bond strength of conventional resin-based adhesive cement and self-adhesive resin cement to CAD-CAM restorative materials. BMC Oral Health. 2025;25:296.
7. Maravić T, Mazzitelli C, Mancuso E, Del Bianco F, Josić U, Cadenaro M, Breschi L, Mazzoni A. Resin composite cements: Current status and a novel classification proposal. J Esthet Restor Dent. 2023;35(7):1085-97.
8. Meharry M, Schwartz J, Montalvo A, Mueller D, Mitchell JC. Comparison of 2 self-adhesive resin cements with or without a self-etching primer. Gen Dent. 2020;68:22-28.
9. Machry RV, Bergoli CD, Schwantz JK, Brondani LP, Pereira-Cenci T, Pereira GK, et al. Longevity of metal-ceramic single crowns cemented onto resin composite prosthetic cores with self-adhesive resin cement: an update of a prospective analysis with up to 106 months of follow-up. Clin Oral Investig. 2023;27:1071-1078. https://doi.org/10.1007/s00784-022-04693-6
10. Özcan M, Bernasconi M. Adhesion to zirconia used for dental restorations: A systematic review and meta-analysis. J Adhes Dent. 2015;17(1):7–26.
11. Yoshida K, Tsuo Y, Atsuta M. Bonding of dual-cured resin cement to zirconia ceramic using phosphate acid ester monomer and zirconate coupler. J Biomed Mater Res B Appl Biomater. 2006;77(1):28–33. https://doi.org/10.1002/jbm.b.30424
12. Kern M. Bonding to oxide ceramics—Laboratory testing versus clinical outcome. Dent Mater. 2015;31(1):8–14. https://doi.org/10.1016/j.dental.2014.06.007
13. Inokoshi M, De Munck J, Minakuchi S, Van Meerbeek B. Meta-analysis of bonding effectiveness to zirconia ceramics. J Dent Res. 2014;93(4):329–334. https://doi.org/10.1177/0022034514524228
14. Grasel R, Santos MJ, Chagas Rêgo HM, Rippe MP, Valandro LF. Effect of Resin Luting Systems and Alumina Particle Air Abrasion on Bond Strength to Zirconia. Oper Dent. 2018;43(3):282-290. https://doi.org/10.2341/15-352-L
15. Blatz MB, Sadan A, Kern M. Resin–ceramic bonding: A review of the literature. J Prosthet Dent. 2003;89(3):268–274. https://doi.org/10.1067/mpr.2003.50
16. Manso AP, Silva NR, Bonfante EA, Pegoraro TA, Dias RA, Carvalho RM. Cements and adhesives for all-ceramic restorations. Dent Clin. 2011;55(2):311-32. https://doi.org/10.1016/j.cden.2011.01.011
17. El Feghaly A, Nasr E, Lukomska-Szymanska M, Zmysłowska-Polakowska E, Najjar G, Harouni R, Bourgi R and Hardan L. Effect of different surface treatments on the bond strength of zirconia to resin cement. An in vitro study. Front. Dent. Med. 2026; 7:1778379. https://doi.org/10.3389/fdmed.2026.1778379
18. Matinlinna JP, Lassila LVJ, Vallittu PK. The effect of five silane coupling agents on the bond strength of a luting cement to a silica-coated titanium. Dent Mater. 2007;23(9):1173–1180. https://doi.org/10.1016/j.dental.2006.06.052
19. Zhang Y, Lawn BR. Novel zirconia materials in dentistry. J Dent Res. 2018;97(2):140–147. https://doi.org/10.1177/0022034517737483
20. Silva LH, Lima E, Miranda RBP, Favero SS, Lohbauer U, Cesar PF. Dental ceramics: A review of new materials and processing methods. Braz Oral Res. 2017;31(suppl 1):e58. https://doi.org/10.1590/1807-3107bor-2017.vol31.0058
21. Motaparthy DS, Ramaraju AV, Alla RK, Bheemalingeswararao D, Sajjan MS, Tanuja D. Evaluation of shear bond strength of self-adhesive resin cements to surface-treated computer-aided design-milled zirconia and lithium disilicate ceramics: an in vitro study. Tanta Dent J. 2025;22(3):468-74.
22. Gomes AL, Castillo-Oyagüe R, Lynch CD, Montero J, Albaladejo A. Influence of sandblasting granulometry and resin cement composition on bonding to zirconia ceramic for dental prosthetic frameworks. J Dent. 2013;41(1):31–41. https://doi.org/10.1016/j.jdent.2012.09.013
23. Teixeira GS, Pereira GKR, Susin AH. Aging methods—an evaluation of their influence on bond strength. Eur J Dent. 2021;15(3):448–45.